(2,4-Dichlorophenyl)boronic acid → HCID 90036840, compound

Participants

Reaction Steps

The title compound, white solid (84 mg, 91%), MS (ISP) m/z=370.4 [(M+H)+], mp 253° C., was prepared in accordance with the general method of example 1 from 7-bromo-1-oxo-2,3,4,5-tetrahydro-[1,4]diazepino[1,2-a]indole-9-carbonitrile (intermediate 20) (76.0 mg, 0.25 mmol) and commercially available 2,4-dichloro-phenylboronic acid (62.0 mg, 0.325 mmol).

Provenance & Evidence