(Pyridin-4-yl)boronic acid → HCID 73335616, compound

Participants

Reaction Steps

The title compound, white solid (29 mg, 38%), MS (ISP) m/z=303.5 [(M+H)+], mp 307° C., was prepared in accordance with the general method of example 1 from 6-bromo-10-methyl-1-oxo-1,2,3,4-tetrahydro-pyrazino[1,2-a]indole-8-carbonitrile (intermediate 16) (76 mg, 0.25 mmol) and commercially available pyridin-4-ylboronic acid (39.9 mg, 0.325 mmol).

Provenance & Evidence