4-tert-Butylphenylboronic acid → HCID 90036362, compound

Participants

Reaction Steps

The title compound, white solid (61 mg, 68%), MS (ISP) m/z=358.5 [(M+H)+], mp 215° C., was prepared in accordance with the general method of example 1 from 7-bromo-1-oxo-2,3,4,5-tetrahydro-[1,4]diazepino[1,2-a]indole-9-carbonitrile (intermediate 20) (76.0 mg, 0.25 mmol) and commercially available 4-tert-butyl-phenylboronic acid (57.9 mg, 0.325 mmol).

Provenance & Evidence