3-Pyridinylboronic acid → HCID 90035928, compound

Participants

Reaction Steps

The title compound, white solid (60 mg, 79%), MS (ISN) m/z=301.4 [(M−H)+], mp 273° C., was prepared in accordance with the general method of example 1 from 6-bromo-10-methyl-1-oxo-1,2,3,4-tetrahydro-pyrazino[1,2-a]indole-8-carbonitrile (intermediate 16) (76 mg, 0.25 mmol) and commercially available pyridin-3-ylboronic acid (39.9 mg, 0.325 mmol).

Provenance & Evidence