3,5-Dichlorophenylboronic acid → HCID 90035811, compound

Participants

Reaction Steps

The title compound, light grey solid (58 mg, 62%), MS (ISN) m/z=368.4 [(M−H)+], mp 347° C., was prepared in accordance with the general method of example 1 from 6-bromo-10-methyl-1-oxo-1,2,3,4-tetrahydro-pyrazino[1,2-a]indole-8-carbonitrile (intermediate 16) (76 mg, 0.25 mmol) and commercially available 3,5-dichloro-phenylboronic acid (62.0 mg, 0.325 mmol).

Provenance & Evidence