HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Bis(benzyloxy)-6-chloropyridazine → HCID 71270197, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Bis(benzyloxy)-6-chloropyridazine | HCID 12213474 | — |
| Reactant | 3,4-bis(Benzyloxy)-6-[(4-fluorophenyl)methyl]pyridazine | HCID 71270427 | — |
| Reactant | HCID 178478034 | HCID 178478034 | — |
| Product | HCID 71270197 | HCID 71270197 | 38% |
Reaction Steps
Prepared as described for 3,4-bis(benzyloxy)-6-[(4-fluorophenyl)methyl]pyridazine (Intermediate 51) from 3,4-bis(benzyloxy)-6-chloropyridazine (Intermediate 1) and (2-chlorobenzyl)zinc(II) chloride in 38% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09290456B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-4844c9959fcc445a9fc30186e42ca730 |
| Source note | uspto-grants-2016_03 |