HuagongsheHuagongshe Chemistry Print Report · For research reference only
(E)-3,4-bis(benzyloxy)-6-(4-(trifluoromethyl)styryl)pyridazine → HCID 178518816, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (E)-3,4-bis(benzyloxy)-6-(4-(trifluoromethyl)styryl)pyridazine | HCID 86677029 | — |
| Reactant | 3-Hydroxy-6-(2-Phenylethyl)pyridazin-4(1h)-One | HCID 178518808 | — |
| Product | HCID 178518816 | HCID 178518816 | — |
Reaction Steps
Prepared by the same method as for 4-hydroxy-6-(2-phenylethyl)pyridazin-3(2H)-one (Example 1) from (E)-3,4-bis(benzyloxy)-6-(4-(trifluoromethyl)styryl)pyridazine (Intermediate 44) except that the product was recrystallised from a mixture of heptane and ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09290456B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-88b08a1f49c04cb7997e5d9ea73b55df |
| Source note | uspto-grants-2016_03 |