(2S)-2-Amino-N,3,3-trimethylbutanamide → HCID 71087306, compound

HRID 927642Notes

Reaction equation

HRID 927642 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([C:8]2[N:13]=[C:12]([C:14]([OH:16])=O)[CH:11]=[CH:10][CH:9]=2)[CH:5]=[CH:6][CH:7]=1.[NH2:17][C@@H:18]([C:23]([CH3:26])([CH3:25])[CH3:24])[C:19]([NH:21][CH3:22])=[O:20]>>[Cl:1][C:2]1[CH:3]=[C:4]([C:8]2[N:13]=[C:12]([C:14]([NH:17][C@@H:18]([C:23]([CH3:26])([CH3:25])[CH3:24])[C:19]([NH:21][CH3:22])=[O:20])=[O:16])[CH:11]=[CH:10][CH:9]=2)[CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 445856(2S)-2-Amino-N,3,3-trimethylbutanamideHCID 247301356-(3-Chlorophenyl)picolinic acid

Product 1

HCID 71087306HCID 71087306, compound

Procedure

The title compound was synthesized in analogy to Example 1, using 6-(3-chlorophenyl)-2-pyridinecarboxylic acid (CAN 863704-38-5) and (2S)-2-amino-N,3,3-trimethyl-butanamide (CAN 89226-12-0) as starting materials, MS (EI): m/e=360.0 [M+H]+.

Sources & evidence

ORD record
ord-a350f3fca191452f94b08653da4a23cc
Source dataset
uspto-grants-2016_03
Patent number
US09290451B2

Reaction notes

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