HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 928129Generated: October 27, 2026
Thionyl Chloride → HCID 86720197, compound
https://huagongshe.com/reaction/928129
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | (1s,4s)-4-(Methoxycarbonyl)-4-methylcyclohexane-1-carboxylic acid | HCID 59133139 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86720197 | HCID 86720197 | — |
Reaction Steps
A solution of 4-(methoxycarbonyl)-4-methylcyclohexanecarboxylic acid (6.67 g, 33.3 mmol) in dichloromethane (30 mL) was charged with thionyl chloride (40 mL, 80 mmol) and then heated to 38° C. for 17 hours. The reaction mixture was cooled to room temperature and then concentrated under reduced pressure to yield methyl 4-(chlorocarbonyl)-1-methylcyclohexanecarboxylate, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09290490B2 |
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| Source dataset | uspto-grants-2016_03 |
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| ORD ID | ord-2fd3c4efce864273a00c7e6ca263f92c |
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| Source note | uspto-grants-2016_03 |
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