HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acryloyl chloride → HCID 86720315, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acryloyl chloride | HCID 13140 | — |
| Reactant | HCID 71226446 | HCID 71226446 | — |
| Product | HCID 86720315 | HCID 86720315 | 26.2% |
Reaction Steps
This compound was prepared, in an analogous manner as described in Example 1, from (S)-4-(8-amino-3-(piperidin-2-yl)imidazo[1,5-a]pyrazin-1-yl)-N-(pyrimidin-2-yl)benzamide (intermediate 27) and acryloylchloride, to afford the title compound (5.9 mg, 26.2%). Data: UPLC(C) Rt: 1.70 min; m/z 469.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09290504B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-bcf2883b59e84b06b7f23bfedb1f85d7 |
| Source note | uspto-grants-2016_03 |