HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Butynoic acid → HCID 71226342, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Butynoic acid | HCID 68535 | — |
| Reactant | HCID 71226349 | HCID 71226349 | — |
| Product | HCID 71226342 | HCID 71226342 | 6.6% |
Reaction Steps
This compound was prepared, in an analogous manner as described in Example 2, from (S)-4-(8-amino-3-(piperidin-2-yl)imidazo[1,5-a]pyrazin-1-yl)-N-(isoxazol-3-yl)benzamide (intermediate 35) and 2-butynoic acid, to afford the title compound (2 mg, 6.6%). Data: UPLC(C) Rt: 2.23 min; m/z 470.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09290504B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-fe5beaea82d24ccfbd4c44c6bb458bbf |
| Source note | uspto-grants-2016_03 |