HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Butynoic acid → HCID 71226747, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Butynoic acid | HCID 68535 | — |
| Reactant | HCID 71225934 | HCID 71225934 | — |
| Product | HCID 71226747 | HCID 71226747 | 59.1% |
Reaction Steps
This compound was prepared, in an analogous manner as described in Example 2, from 4-(8-amino-3-((S)-piperidin-2-yl)imidazo[1,5-a]pyrazin-1-yl)-3-methyl-N-(pyridin-2-yl)benzamide (intermediate 43) and 2-butynoic acid, to afford the title compound (13.7 mg, 59.1%). Data: UPLC(C) Rt: 2.28 min; m/z 494.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09290504B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-01b3248d83794ea2898300822da9cf7d |
| Source note | uspto-grants-2016_03 |