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(S)-4-(8-Amino-3-(pyrrolidin-2-yl)imidazo[1,5-a]pyrazin-1-yl)-N-(pyridin-2-yl)benzamide → HCID 86720323、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (S)-4-(8-Amino-3-(pyrrolidin-2-yl)imidazo[1,5-a]pyrazin-1-yl)-N-(pyridin-2-yl)benzamide | HCID 71226368 | — |
| 溶媒 | 2-Pentynoic acid | HCID 324379 | — |
| 生成物 | HCID 86720323 | HCID 86720323 | 24.7% |
反応手順
This compound was prepared, in an analogous manner as described in Example 2, from the compound described in intermediate 2b and pent-2-ynoic acid, to afford the title compound (7.4 mg, 24.7%). Data: UPLC (C) Rt: 1.73 min; m/z 480.3 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09290504B2 |
| 出典データセット | uspto-grants-2016_03 |
| ORD ID | ord-0747073207714c25bffff2d57bea7b6b |
| 出典メモ | uspto-grants-2016_03 |