HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acryloyl chloride → HCID 78131162, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acryloyl chloride | HCID 13140 | — |
| Reactant | HCID 71226846 | HCID 71226846 | — |
| Product | HCID 78131162 | HCID 78131162 | 32.6% |
Reaction Steps
This compound was prepared, in an analogous manner as described in Example 1, from 4-(8-amino-3-(azepan-2-yl)imidazo[1,5-a]pyrazin-1-yl)-N-(pyridin-2-yl)benzamide (intermediate 46) and acryloylchloride, to afford the title compound (11 mg, 32.6%). Data: UPLC(C) Rt: 1.88 min; m/z 482.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09290504B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-1101832680bd494fa1d0ae7508945a84 |
| Source note | uspto-grants-2016_03 |