HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Butynoic acid → HCID 71226641, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Butynoic acid | HCID 68535 | — |
| Reactant | HCID 86720324 | HCID 86720324 | — |
| Product | HCID 71226641 | HCID 71226641 | 33.4% |
Reaction Steps
This compound was prepared, in an analogous manner as described in Example 2, from (S)-4-(8-amino-3-(1-(methylamino)ethyl)imidazo[1,5-a]pyrazin-1-yl)-N-(4-(trifluoromethyl)pyridin-2-yl)benzamide (intermediate 48) and 2-butynoic acid, to afford the title compound (11.5 mg, 33.4%). Data: UPLC(C) Rt: 2.54 min; m/z 522.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09290504B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-c15a9ad80dc24d5788c7eb040db5fb14 |
| Source note | uspto-grants-2016_03 |