HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Butynoic acid, 4-methoxy- → HCID 71226583, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Butynoic acid, 4-methoxy- | HCID 11126213 | — |
| Reactant | (S)-4-(8-Amino-3-(pyrrolidin-2-yl)imidazo[1,5-a]pyrazin-1-yl)-N-(pyridin-2-yl)benzamide | HCID 71226368 | — |
| Product | HCID 71226583 | HCID 71226583 | 24.7% |
Reaction Steps
This compound was prepared, in an analogous manner as described in Example 2, from the compound described in intermediate 2b and 4-methoxybut-2-ynoic acid (Intermediate 50), to afford the title compound (9.1 mg, 24.7%). Data: UPLC (C) Rt: 1.44 min; m/z 496.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09290504B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-5298624521e04018be0e7cd8da9f9a83 |
| Source note | uspto-grants-2016_03 |