HRID928428

反应详情

EQUATION

反应方程式

HRID 928428 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

CONDITIONS

反应条件

温度
20 °C

PROCEDURE

实验过程

Ethyl 1-((1-methyl-1,2,3,4-tetrahydroquinolin-7-yl)methyl)-1H-pyrazole-4-carboxylate (233 mg, 0.607 mmol) was dissolved in a mixture of MeOH (6 ml) and 1N NaOH (3.00 ml). The reaction mixture was stirred for 8 hr at 20° C. and the solvents were removed by evaporation under reduced pressure to afford the title compound. HPLC (Method A) Rt=1.348 min; MS (Method A) [M+H]+=271.9

WORKUP

后处理

  1. customthe solvents were removed by evaporation under reduced pressure