Sodium Azide → HCID 58081357, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of 2-(bromomethyl)-7-chloroquinoline (50 mg, 0.195 mmol) in DMF (0.5 ml) was added sodium azide (19.01 mg, 0.292 mmol). Reaction mixture was stirred for 2 h at 90° C. Reaction mixture was diluted with ethyl acetate/water. Layers were separated and organic layer was washed twice with water and with brine, dried over sodium sulfate, filtered and evaporated to afford the title compound. HPLC (Method G) Rt=1.990 min, MS (Method V) [M+H]+=219.1.

Provenance & Evidence