Dichloromethane → HCID 58081249, compound

Participants

Reaction Steps

To a solution of tent-Butyl 5-((1-((3-chloroquinolin-6-yl)methyl)-1H-pyrazole-4-carboxamido)methyl)-4,6-dimethylpyridin-2-ylcarbamate (125 mg, 0.240 mmol) in DCM (1 ml) Tri fluoro acetic acid (0.092 ml, 1.200 mmol) was added at rt. The reaction was stirred for 2 h at II. The reaction mixture was concentrated under vacuum to afford crude title compound. The crude product was dissolved in MeOH and filtered over a PL-HCO3-cartridge (MP-resin, VARIAN) to afford pure title compound.

Provenance & Evidence