3-Chlorobenzaldehyde → 5-(3-Chlorobenzyl)-2,2-dimethyl-1,3-dioxane-4,6-dione

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Reaktionsgleichung

[Cl:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][CH:9]=1)[CH:5]=O.ClC1C=CC(C[CH:16]2[C:21](=[O:22])[O:20][C:19]([CH3:24])([CH3:23])[O:18][C:17]2=[O:25])=CC=1.BrC1C=C2C(=CC=1)N=C(Cl)C(CC1C=CC(Cl)=CC=1)=C2Cl>>[Cl:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][CH:9]=1)[CH2:5][CH:16]1[C:21](=[O:22])[O:20][C:19]([CH3:24])([CH3:23])[O:18][C:17]1=[O:25]

Komponenten

Edukt 3

HCID 114773-Chlorobenzaldehyde

HCID 108801105-(4-Chlorobenzyl)-2,2-dimethyl-1,3-dioxane-4,6-dione

HCID 867155806-Bromo-2,4-dichloro-3-(4-chlorobenzyl)quinoline

Produkt 1

HCID 110000795-(3-Chlorobenzyl)-2,2-dimethyl-1,3-dioxane-4,6-dione

Versuchsvorschrift

The title compound was prepared using 3-chlorobenzaldehyde in place of 4-chlorobenzaldehyde using the procedure described for the preparation of 5-(4-chlorobenzyl)-2,2-dimethyl-1,3-dioxane-4,6-dione (Intermediate 3: step a).

Quellen und Nachweise

ORD-Eintrag: ord-41e271a986dd46718c1b0585b7ee8353
Quelldatensatz: uspto-grants-2016_03
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US09290476B2

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