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4-(Methylsulfonyl)benzaldehyde → 5-(4-Methylsulfonylbenzyl)-2,2-dimethyl-1,3-dioxane-4,6-dione
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-(Methylsulfonyl)benzaldehyde | HCID 220376 | — |
| 反応物 | 5-(4-Chlorobenzyl)-2,2-dimethyl-1,3-dioxane-4,6-dione | HCID 10880110 | — |
| 反応物 | 6-Bromo-2,4-dichloro-3-(4-chlorobenzyl)quinoline | HCID 86715580 | — |
| 生成物 | 5-(4-Methylsulfonylbenzyl)-2,2-dimethyl-1,3-dioxane-4,6-dione | HCID 86715585 | — |
反応手順
The title compound was prepared using 4-(methylsulfonyl)benzaldehyde in place of 4-chlorobenzaldehyde using the procedure described for the preparation of 5-(4-chlorobenzyl)-2,2-dimethyl-1,3-dioxane-4,6-dione (Intermediate 3: step a).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09290476B2 |
| 出典データセット | uspto-grants-2016_03 |
| ORD ID | ord-16fecc90e8f0405a93067b20fb591785 |
| 出典メモ | uspto-grants-2016_03 |