HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-4-fluorophenylhydrazine hydrochloride → HCID 89610063, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-4-fluorophenylhydrazine hydrochloride | HCID 44181777 | — |
| Reactant | 5-(3-Chloro-5-fluorophenyl)-1-(pyridin-2-yl)-1H-pyrazole-3-carboxylic acid | HCID 89602575 | — |
| Reactant | HCID 131735140 | HCID 131735140 | — |
| Product | HCID 89610063 | HCID 89610063 | — |
Reaction Steps
240 mg (0.86 mmol) of the compound of Example 15A is reacted analogously to the synthesis of the compound of Example 20A with 253 mg (1.29 mmol) of 3-chloro-4-fluorophenylhydrazine hydrochloride. After hydrolysis, 16 mg (5% of theory) of the title compound is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09296720B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-f7d81e8b91a14e84a254b39089fa6c76 |
| Source note | uspto-grants-2016_03 |