HRID930040

反应详情

EQUATION

反应方程式

HRID 930040 的结构方程式

PROCEDURE

实验过程

600 mg (1.33 mmol) of the compound of Example 16A is reacted analogously to the synthesis of the compound of Example 20A with 288 mg (1.46 mmol) of 3-chloro-4-fluorophenylhydrazine hydrochloride. After hydrolysis, the entire reaction mixture is reduced to the dry state i. vac. 712 mg (37% purity, 57% of theory) of the title compound, which is used without further purification, is obtained.

WORKUP

后处理

  1. customAfter hydrolysis
  2. customthe entire reaction mixture
  3. custom712 mg (37% purity, 57% of theory) of the title compound, which is used without further purification
  4. customis obtained