HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-chloropyridine N-oxide → HCID 68657451, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-chloropyridine N-oxide | HCID 70724 | — |
| Reactant | (4-Fluoro-2-methoxyphenyl)boronic acid | HCID 2782672 | — |
| Product | HCID 68657451 | HCID 68657451 | 87.4% |
Reaction Steps
4-Chloropyridine-N-oxide (305 mg, 2.35 mmol), 4-fluoro-2-methoxyphenylboronic acid (1.0 g, 8.8 mmol) were reacted according to the procedure of Example 39 (step a) to provide the title compound (450 mg, 87%) as a purple solid: 1H NMR (300 MHz, CDCl3) δ 8.21 (d, J=7.2 Hz, 2H), 7.45 (d, J=7.2 Hz, 2H), 7.31 (d, J=6.5 Hz, 1H), 6.80-6.71 (m, 2H), 3.85 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09296743B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-d07b150ff61b439ca997b923dbaf8ff5 |
| Source note | uspto-grants-2016_03 |