5-Bromo-2-(trifluoromethyl)pyridine → HCID 57514758, compound

Participants

Role	Name	HCID	Charge
Reactant	5-Bromo-2-(trifluoromethyl)pyridine	HCID 2761197	—
Reactant	2-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine	HCID 44754862	—
Product	HCID 57514758	HCID 57514758	816.4%

Reaction Steps

2-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine (1.24 g, 0.53 mmol) and 5-bromo-2-(trifluoromethyl)pyridine (2.4 g, 11 mmol) were reacted according to the procedure of Example 31 (step a) to provide the title compound (1.1 g, 81%) as a white solid: ESI MS m/z 255 [M+H].

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US09296743B2
Source dataset	uspto-grants-2016_03
ORD ID	ord-0aefc8cb2414419cbd5382748ab68a9e
Source note	uspto-grants-2016_03