HCID 71616298, compound → HCID 86721052, compound

HRID 930867Notes

Reaction equation

HRID 930867 reaction equation
[F:1][C:2]1([F:29])[CH2:7][CH2:6][CH:5]([O:8][C:9]2[CH:14]=[CH:13][C:12]([N+:15]([O-])=O)=[CH:11][C:10]=2[C:18]2[C:19]3[CH:28]=[CH:27][NH:26][C:20]=3[C:21](=[O:25])[N:22]([CH3:24])[CH:23]=2)[CH2:4][CH2:3]1.CN1C=C(C2C=C([N+]([O-])=O)C=CC=2OC2C=CC=CC=2)C2C=CNC=2C1=O>>[NH2:15][C:12]1[CH:13]=[CH:14][C:9]([O:8][CH:5]2[CH2:4][CH2:3][C:2]([F:1])([F:29])[CH2:7][CH2:6]2)=[C:10]([C:18]2[C:19]3[CH:28]=[CH:27][NH:26][C:20]=3[C:21](=[O:25])[N:22]([CH3:24])[CH:23]=2)[CH:11]=1

Participants

3

Reactant 2

HCID 71616298HCID 71616298, compoundHCID 86721053HCID 86721053, compound

Product 1

HCID 86721052HCID 86721052, compound

Procedure

Example 59b was prepared according to the procedure used for the preparation of Example 3, substituting the product of Example 59a for the product of Example 2b, to provide the title compound.

Workup

  1. customExample 59b was prepared
  2. customused for the preparation of Example 3

Sources & evidence

ORD record
ord-ac0fdebfec804969a7995d0d21b2e206
Source dataset
uspto-grants-2016_03
Patent number
US09296741B2

Reaction notes

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