HCID 86721037, compound → HCID 86721054, compound
Reaction equation
[CH3:1][N:2]1[CH:7]=[C:6]([C:8]2[CH:13]=[C:12]([N+:14]([O-])=O)[CH:11]=[CH:10][C:9]=2[O:17][CH:18]2[CH2:23][CH2:22][CH2:21][O:20][CH2:19]2)[C:5]2[CH:24]=[CH:25][NH:26][C:4]=2[C:3]1=[O:27].CN1C=C(C2C=C([N+]([O-])=O)C=CC=2OC2CCOCC2)C2C=CNC=2C1=O>>[NH2:14][C:12]1[CH:11]=[CH:10][C:9]([O:17][CH:18]2[CH2:23][CH2:22][CH2:21][O:20][CH2:19]2)=[C:8]([C:6]2[C:5]3[CH:24]=[CH:25][NH:26][C:4]=3[C:3](=[O:27])[N:2]([CH3:1])[CH:7]=2)[CH:13]=1Participants
3
Procedure
Example 60b was prepared according to the procedure used for the preparation of Example 29b, substituting the product of Example 60a for the product of Example 29a, to provide the title compound.
Workup
- customExample 60b was prepared
- customused for the preparation of Example 29b
Sources & evidence
- ORD record
- ord-c6dad59c77ff48eea52f8140ca489a0f
- Source dataset
- uspto-grants-2016_03
- Patent number
- US09296741B2
Reaction notes
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