HCID 71616298, compound → HCID 86721066, compound

HRID 930902Notes

Reaction equation

HRID 930902 reaction equation
[CH:1]1([CH2:4][O:5][C:6]2[C:11]([C:12]3[C:13]4[CH:22]=[CH:21][N:20]([S:23]([C:26]5[CH:32]=[CH:31][C:29]([CH3:30])=[CH:28][CH:27]=5)(=[O:25])=[O:24])[C:14]=4[C:15](=[O:19])[N:16]([CH3:18])[CH:17]=3)=[C:10]([CH3:33])[C:9]([N+:34]([O-])=O)=[CH:8][CH:7]=2)[CH2:3][CH2:2]1.CN1C=C(C2C=C([N+]([O-])=O)C=CC=2OC2C=CC=CC=2)C2C=CNC=2C1=O>>[NH2:34][C:9]1[C:10]([CH3:33])=[C:11]([C:12]2[C:13]3[CH:22]=[CH:21][N:20]([S:23]([C:26]4[CH:27]=[CH:28][C:29]([CH3:30])=[CH:31][CH:32]=4)(=[O:25])=[O:24])[C:14]=3[C:15](=[O:19])[N:16]([CH3:18])[CH:17]=2)[C:6]([O:5][CH2:4][CH:1]2[CH2:2][CH2:3]2)=[CH:7][CH:8]=1

Participants

3

Reactant 2

HCID 71616298HCID 71616298, compoundHCID 86721067HCID 86721067, compound

Product 1

HCID 86721066HCID 86721066, compound

Procedure

Example 251c was prepared according to the procedure used for the preparation of Example 3, substituting the product of Example 251b for the product of Example 2b to provide the title compound.

Workup

  1. customExample 251c was prepared
  2. customused for the preparation of Example 3

Sources & evidence

ORD record
ord-d140c425618745dd8ab277d14d053b49
Source dataset
uspto-grants-2016_03
Patent number
US09296741B2

Reaction notes

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