HCID 71616298, compound → HCID 86721068, compound

HRID 930907Notes

Reaction equation

HRID 930907 reaction equation
[CH:1]1([CH2:4][O:5][C:6]2[CH:11]=[C:10]([CH3:12])[C:9]([N+:13]([O-])=O)=[CH:8][C:7]=2[C:16]2[C:17]3[CH:26]=[CH:25][N:24]([S:27]([C:30]4[CH:36]=[CH:35][C:33]([CH3:34])=[CH:32][CH:31]=4)(=[O:29])=[O:28])[C:18]=3[C:19](=[O:23])[N:20]([CH3:22])[CH:21]=2)[CH2:3][CH2:2]1.CN1C=C(C2C=C([N+]([O-])=O)C=CC=2OC2C=CC=CC=2)C2C=CNC=2C1=O>>[NH2:13][C:9]1[C:10]([CH3:12])=[CH:11][C:6]([O:5][CH2:4][CH:1]2[CH2:3][CH2:2]2)=[C:7]([C:16]2[C:17]3[CH:26]=[CH:25][N:24]([S:27]([C:30]4[CH:36]=[CH:35][C:33]([CH3:34])=[CH:32][CH:31]=4)(=[O:29])=[O:28])[C:18]=3[C:19](=[O:23])[N:20]([CH3:22])[CH:21]=2)[CH:8]=1

Participants

3

Reactant 2

HCID 71616298HCID 71616298, compoundHCID 86721069HCID 86721069, compound

Product 1

HCID 86721068HCID 86721068, compound

Procedure

Example 263c was prepared according to the procedure used for the preparation of Example 3, substituting the product of Example 263b for the product of Example 2b to provide the title compound.

Workup

  1. customExample 263c was prepared
  2. customused for the preparation of Example 3

Sources & evidence

ORD record
ord-87d9fc239bce4923a8989518135f686c
Source dataset
uspto-grants-2016_03
Patent number
US09296741B2

Reaction notes

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