HCID 89853412, compound → HCID 89852907, compound

HRID 931082Notes

Reaction equation

HRID 931082 reaction equation
[CH2:1]([O:3][C:4](=[NH:18])[C:5]1[CH:6]=[C:7]([CH:13]=[C:14](OC)[N:15]=1)[C:8]([O:10][CH2:11][CH3:12])=[O:9])[CH3:2].Cl[C:20]1[CH:21]=C(C=C(CC)N=1)C(OCC)=O>>[CH2:1]([O:3][C:4](=[NH:18])[C:5]1[CH:6]=[C:7]([CH:13]=[C:14]([CH2:20][CH3:21])[N:15]=1)[C:8]([O:10][CH2:11][CH3:12])=[O:9])[CH3:2]

Participants

3

Reactant 2

HCID 89853412HCID 89853412, compoundHCID 89853650HCID 89853650, compound

Product 1

HCID 89852907HCID 89852907, compound

Procedure

The title compound was prepared by a method analogous to Intermediate 17 but using ethyl 2-chloro-6-ethylisonicotinate as the starting material. GCMS analysis of the reaction mixture showed the presence of the desired product. MS (EI+) (M+) 250; GCMS retention time 3.611 minutes (Method O).

Sources & evidence

ORD record
ord-c271697c40a74c289e5182866bc0f496
Source dataset
uspto-grants-2016_03
Patent number
US09296745B2

Reaction notes

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