HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 3-(4-Bromophenyl)propanoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-(4-Bromophenyl)propionic acid | HCID 2735609 | — |
| Product | 3-(4-Bromophenyl)propanoyl chloride | HCID 22411651 | 99% |
Reaction Steps
A solution of 3-(4-bromophenyl)propanoic acid (14.5 g, 63.60 mmol, 1.00 equiv) in thionyl chloride (80 mL) was refluxed for 2 h. The reaction mixture was cooled to room temperature and then concentrated under vacuum to give 15.5 g (99%) of 3-(4-bromophenyl)propanoyl chloride as a light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09296732B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-8b8fbb5e33db44c8b1d88be70659b201 |
| Source note | uspto-grants-2016_03 |