HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-Chloro-5-(4-chlorophenyl)-2-methyl-6-vinylquinoline → 5-(4-Chlorophenyl)-2,7-dimethyl-6-vinylquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-Chloro-5-(4-chlorophenyl)-2-methyl-6-vinylquinoline | HCID 66630622 | — |
| Reactant | 5-(4-Chlorophenyl)-2,7-dimethylquinolin-6-yl trifluoromethanesulfonate | HCID 86691974 | — |
| Product | 5-(4-Chlorophenyl)-2,7-dimethyl-6-vinylquinoline | HCID 66631776 | — |
Reaction Steps
Compound 2F was prepared following the procedure used to prepare compound 1G of Example 1, except that 5-(4-chlorophenyl)-2,7-dimethylquinolin-6-yl trifluoromethanesulfonate (2E) was used instead of compound 1F. LCMS-ESI+ (m/z): 294.3, 296.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09296758B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-945547565c784412803c9da448e9b2b4 |
| Source note | uspto-grants-2016_03 |