HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-7-methyl-2-(trifluoromethyl)quinolin-6-ol → 5-Bromo-7-methyl-2-(trifluoromethyl)quinolin-6-yl trifluoromethanesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-7-methyl-2-(trifluoromethyl)quinolin-6-ol | HCID 66631612 | — |
| Reactant | 7-Chloro-5-(4-chlorophenyl)-2-methylquinolin-6-yl trifluoromethanesulfonate | HCID 86691972 | — |
| Product | 5-Bromo-7-methyl-2-(trifluoromethyl)quinolin-6-yl trifluoromethanesulfonate | HCID 86691978 | — |
Reaction Steps
Compound 7C was prepared following the procedure used to prepare compound 1F of Example 1 except that 5-bromo-7-methyl-2-(trifluoromethyl)quinolin-6-ol (7B) was used instead of compound 1E. LCMS-ESI+ (m/z): 437.8, 439.8 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09296758B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-6c24469a56ea4520ae5e1644d8f98161 |
| Source note | uspto-grants-2016_03 |