HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2,7-dimethyl-6-vinylquinoline → 5-Bromo-7-methyl-2-(trifluoromethyl)-6-vinylquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2,7-dimethyl-6-vinylquinoline | HCID 66631391 | — |
| Reactant | 5-Bromo-7-methyl-2-(trifluoromethyl)quinolin-6-yl trifluoromethanesulfonate | HCID 86691978 | — |
| Product | 5-Bromo-7-methyl-2-(trifluoromethyl)-6-vinylquinoline | HCID 66631804 | — |
Reaction Steps
Compound 7D was prepared following the procedure used to prepare compound 5B of Example 5, except that 5-bromo-7-methyl-2-(trifluoromethyl)quinolin-6-yl trifluoromethanesulfonate (7C) was used instead of compound 5A. LCMS-ESI+ (m/z): 316.1, 318.1 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09296758B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-0b1e9fd34bdd4061a50785c79f85dbbf |
| Source note | uspto-grants-2016_03 |