HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66631444, compound → HCID 66631878, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66631444 | HCID 66631444 | — |
| Reactant | HCID 66631448 | HCID 66631448 | — |
| Reactant | (S)-2-tert-butoxy-2-(5-(4-chlorophenyl)-7-methyl-2-(trifluoromethylsulfonyloxy)quinolin-6-yl)ethyl pivalate | HCID 86691982 | — |
| Product | HCID 66631878 | HCID 66631878 | — |
Reaction Steps
(S)-2-tert-Butoxy-2-(5-(4-chlorophenyl)-2-cyclopropyl-7-methylquinolin-6-yl)ethanol was prepared following the procedure used to prepare compound (S)-2-tert-butoxy-2-(5-(4-chlorophenyl)-7-methyl-2-vinylquinolin-6-yl)ethanol, (compound of Example 26) except that (S)-2-tert-butoxy-2-(5-(4-chlorophenyl)-2-cyclopropyl-7-methylquinolin-6-yl)ethyl pivalate was used instead of (S)-2-tert-butoxy-2-(5-(4-chlorophenyl)-7-methyl-2-vinylquinolin-6-yl)ethyl pivalate. LCMS-ESI+ (m/z): 410.3, 412.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09296758B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-b83a086635fd40efb6dbfa4aeb59b6d4 |
| Source note | uspto-grants-2016_03 |