HRID931881

反应详情

EQUATION

反应方程式

HRID 931881 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
85 °C

PROCEDURE

实验过程

Thereafter, a mixture of 66.88 parts by mass of acrylic acid and 53.27 parts by mass of methacrylic acid, and a solution of 15.49 parts by mass of 2,2′-azobis[2-(2-imidazolin-2-yl)propane] and 12.14 parts by mass of concentrated sulfuric acid dissolved in 80.00 parts by mass of deionized water, were simultaneously poured into the flask over 60 minutes. The mixture was kept warm at 85° C. for 2 hours to complete the polymerization reaction, and then the resultant was cooled and taken out. Thus, an acrylic acid/methacrylic acid copolymer was obtained. The non-volatile component fraction was measured, and it was 40% by mass. Furthermore, the molecular weight of the acrylic acid/methacrylic acid copolymer thus obtained was measured by the method described above, and the weight average molecular weight was 8,900 (relative to polyethylene glycol standards).

WORKUP

后处理

  1. additionwere simultaneously poured into the flask over 60 minutes
  2. customthe polymerization reaction
  3. temperaturethe resultant was cooled