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HRID931922

反应详情

EQUATION

反应方程式

HRID 931922 的结构方程式

REACTANTS

反应物

2
结构：BrCC1CCCC1
HCID12723264

(Bromomethyl)cyclopentane

C6H11Br

结构：C=CC[C@@H]1C[C@H](c2cccc(Cl)c2)[C@@H](c2ccc(Cl)cc2)NC1=O
HCID58573283

未命名化合物

PRODUCTS

生成物

1
结构：C=CC[C@@H]1C[C@H](c2cccc(Cl)c2)[C@@H](c2ccc(Cl)cc2)N(CC2CCCC2)C1=O
HCID67999125

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from (3R,5R,6S)-3-allyl-5-(3-chlorophenyl)-6-(4-chlorophenyl)piperidin-2-one (Example 42, Step A) and (bromomethyl)cyclopentane as described in Example 44, Step A. Purification of the residue by silica gel prep plate (25% EtOAc/hexanes) provided the title compound as a colorless solid.

WORKUP

后处理

  1. customPurification of the residue by silica gel prep plate (25% EtOAc/hexanes)