Propanal → HCID 67999216, compound

HRID 932182Notes

Reaction equation

HRID 932182 reaction equation
Br[C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([C:8]([F:11])([F:10])[F:9])[N:3]=1.[CH:12](=[O:15])[CH2:13][CH3:14].N1C=CC=CC=1C(O)CCC>>[F:9][C:8]([F:11])([F:10])[C:4]1[N:3]=[C:2]([CH:12]([OH:15])[CH2:13][CH3:14])[CH:7]=[CH:6][CH:5]=1

Participants

4

Reactant 3

HCID 527PropanalHCID 27829022-Bromo-6-(trifluoromethyl)pyridineHCID 13926171HCID 13926171, compound

Product 1

HCID 67999216HCID 67999216, compound

Procedure

The title compound was prepared from 2-bromo-6-(trifluoromethyl)pyridine (purchased from Oakwood Products Inc., West Columbia, S.C.) and propionaldehyde following the procedure as described above for the synthesis of 1-(pyridin-2-yl)butan-1-ol (Example 231, Step A). Mass Spectrum (ESI) m/z=206.1 (M+1).

Sources & evidence

ORD record
ord-2714b477974e45fe8b703ac592d7336e
Source dataset
uspto-grants-2016_03
Patent number
US09296736B2

Reaction notes

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