Acetate → 7-Methoxy-2-oxo-1,2,4,5-tetrahydrobenzo[d]azepine-3-carboxylic acid benzyl ester

HRID 934655Notes

Reaction equation

HRID 934655 reaction equation
[C:24]([O-:25])(=[O:26])[CH3:27].[C:28]([O-:29])(=[O:30])[CH3:31].[C:32]([O-:33])(=[O:34])[CH3:35].[C:36]([O-:37])(=[O:38])[CH3:39].[CH2:1]([c:2]1[cH:3][cH:4][cH:5][cH:6][cH:7]1)[O:8][C:9](=[O:10])[N:11]1[C:12](=[CH2:23])[c:13]2[cH:14][cH:15][c:16]([O:21][CH3:22])[cH:17][c:18]2[CH2:19][CH2:20]1.[CH3:41][C:42](=[O:43])[OH:44].[Pb+4:40]>>[CH2:1]([c:2]1[cH:3][cH:4][cH:5][cH:6][cH:7]1)[O:8][C:9](=[O:10])[N:11]1[C:12](=[O:26])[CH2:23][c:13]2[cH:14][cH:15][c:16]([O:21][CH3:22])[cH:17][c:18]2[CH2:19][CH2:20]1

Participants

5

Reactant 4

HCID 175Acetate4×HCID 176Acetic AcidHCID 138591896-methoxy-1-methylene-3,4-dihydro-1H-isoquinoline-2-carboxylic acid benzyl esterHCID 178527690HCID 178527690, compound

Product 1

HCID 235442487-Methoxy-2-oxo-1,2,4,5-tetrahydrobenzo[d]azepine-3-carboxylic acid benzyl ester

Sources & evidence

ORD record
ord-c2c40c55b5794207ad8c2e5931f954c7
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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