Potassium Cation → tert-Butyl 4-(prop-2-yn-1-yl)piperazine-1-carboxylate

HRID 934730Notes

Reaction equation

HRID 934730 reaction equation
[C:18](=[O:19])([O-:20])[O-:21].[C:1]([CH3:2])([CH3:3])([CH3:4])[O:5][C:6](=[O:7])[N:8]1[CH2:9][CH2:10][NH:11][CH2:12][CH2:13]1.[CH2:14]([C:15]#[CH:16])[Br:17].[CH3:24][C:25]#[N:26].[Cl:27][CH2:28][Cl:29].[K+:22].[K+:23]>>[C:1]([CH3:2])([CH3:3])([CH3:4])[O:5][C:6](=[O:7])[N:8]1[CH2:9][CH2:10][N:11]([CH2:16][C:15]#[CH:14])[CH2:12][CH2:13]1

Participants

7

Reactant 6

HCID 813Potassium Cation2×HCID 6342AcetonitrileHCID 6344DichloromethaneHCID 7842Propargyl bromideHCID 19660Carbonate IonHCID 143452tert-Butyl piperazine-1-carboxylate

Product 1

HCID 11287538tert-Butyl 4-(prop-2-yn-1-yl)piperazine-1-carboxylate

Sources & evidence

ORD record
ord-de8fa6dc559943fc9e1aad7bfbdce83a
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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