HRID9363

反应详情

EQUATION

反应方程式

HRID 9363 的结构方程式

PROCEDURE

实验过程

4—Chloro-3-nitro-7-phenylquinoline (5.3 g, 18.8 mmol) and 3-methylsulfanyl-propylamine (2.17 g, 20.6 mmol) were combined and treated according to the general procedure described in Part E of Example 1. Recrystallization from isopropanol afforded 6.2 g of (3-methylsulfanylpropyl)-(3-nitro-7-phenylquinolin-4-yl)amine as gold plates.

WORKUP

后处理

  1. additiontreated
  2. customRecrystallization from isopropanol