HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → 3,4,4-Trifluoro-3-butenoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 3,4,4-Trifluoro-3-butenoic acid | HCID 15239174 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Product | 3,4,4-Trifluoro-3-butenoyl chloride | HCID 10920789 | — |
Reaction Steps
Reaction of 3,4,4-trifiuoro-3-butenoic acid (IV) with oxalyl chloride in the presence of DMF as a catalyst without any solvent to give 3,4,4-trifluoro-3-butenoyl chloride (V).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05723470 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-c52267ccc4ea462db1460373af993a7c |
| Source note | uspto-grants-1998_03 |