Methanol → Methyl 2-amino-5-(benzyloxy)-4-methoxybenzoate

HRID 945740Notes

Reaction equation

HRID 945740 reaction equation
[CH2:1]([c:2]1[cH:3][cH:4][cH:5][cH:6][cH:7]1)[O:8][c:9]1[c:10]([O:22][CH3:23])[cH:11][c:12]([N+:19]([O-:20])=[O:21])[c:13]([C:14](=[O:15])[O:16][CH3:17])[cH:18]1.[CH3:32][OH:33].[Na+:30].[Na+:31].[OH2:34].[S:24]([S:25]([O-:26])=[O:27])([O-:28])=[O:29]>>[CH2:1]([c:2]1[cH:3][cH:4][cH:5][cH:6][cH:7]1)[O:8][c:9]1[c:10]([O:22][CH3:23])[cH:11][c:12]([NH2:19])[c:13]([C:14](=[O:15])[O:16][CH3:17])[cH:18]1

Participants

6

Reactant 5

HCID 887MethanolHCID 923Sodium ion2×HCID 962WaterHCID 1086DithioniteHCID 22667156Methyl 5-Benzyloxy-4-methoxy-2-nitrobenzoate

Product 1

HCID 22667093Methyl 2-amino-5-(benzyloxy)-4-methoxybenzoate

Sources & evidence

ORD record
ord-5212b6d1e57645f5b5059d760243ecbc
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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