Methanol → Di-tert-butyl 2-(2-oxopiperazin-1-yl)ethyl phosphate

HRID 946720Notes

Reaction equation

HRID 946720 reaction equation
[C:1]([CH3:2])([CH3:3])([CH3:4])[O:5][P:6](=[O:7])([O:8][C:9]([CH3:10])([CH3:11])[CH3:12])[O:13][CH2:14][CH2:15][N:16]1[C:17](=[O:32])[CH2:18][N:19]([C:22]([O:23][CH2:24][c:25]2[cH:26][cH:27][cH:28][cH:29][cH:30]2)=[O:31])[CH2:20][CH2:21]1.[CH3:35][OH:36].[H:33][H:34]>>[C:1]([CH3:2])([CH3:3])([CH3:4])[O:5][P:6](=[O:7])([O:8][C:9]([CH3:10])([CH3:11])[CH3:12])[O:13][CH2:14][CH2:15][N:16]1[C:17](=[O:32])[CH2:18][NH:19][CH2:20][CH2:21]1

Participants

4

Reactant 3

HCID 887MethanolHCID 68638741Benzyl 4-{2-[(di-tert-butoxyphosphoryl)oxy]ethyl}-3-oxopiperazine-1-carboxylateHCID 178418361HCID 178418361, compound

Product 1

HCID 68640146Di-tert-butyl 2-(2-oxopiperazin-1-yl)ethyl phosphate

Sources & evidence

ORD record
ord-59e9aacdde6e4c8e8fb3f8c88d439bad
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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