Diethyl Ether → Methyl 3-butyl-1-formylcyclobutane-1-carboxylate

HRID 957296Notes

Reaction equation

HRID 957296 reaction equation
[CH2:18]([Al+:19][CH2:20][CH:21]([CH3:22])[CH3:23])[CH:24]([CH3:25])[CH3:26].[CH3:1][O:2][C:3](=[O:4])[C:5]1([C:13](=[O:14])[O:15][CH3:16])[CH2:6][CH:7]([CH2:9][CH2:10][CH2:11][CH3:12])[CH2:8]1.[CH3:27][CH2:28][O:29][CH2:30][CH3:31].[H-:17]>>[CH3:1][O:2][C:3](=[O:4])[C:5]1([CH:13]=[O:14])[CH2:6][CH:7]([CH2:9][CH2:10][CH2:11][CH3:12])[CH2:8]1

Participants

5

Reactant 4

HCID 3283Diethyl EtherHCID 166653HydrideHCID 16686348Bis(2-methylpropyl)alumanyliumHCID 69222797Dimethyl 3-butylcyclobutane-1,1-dicarboxylate

Product 1

HCID 71416977Methyl 3-butyl-1-formylcyclobutane-1-carboxylate

Sources & evidence

ORD record
ord-f0719dd71d43458d8270fd8485061b71
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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