Dichloromethane → tert-Butyl 4-formylpiperidine-1-carboxylate

HRID 961781Notes

Reaction equation

HRID 961781 reaction equation
[C:1](=[O:2])([O:3][C:4]([CH3:5])([CH3:6])[CH3:7])[N:8]1[CH2:9][CH2:10][CH:11]([CH2:14][OH:15])[CH2:12][CH2:13]1.[Cl:27][CH2:28][Cl:29].[O:16]=[Cr:17]([Cl:18])([O-:19])=[O:20].[nH+:21]1[cH:22][cH:23][cH:24][cH:25][cH:26]1>>[C:1](=[O:2])([O:3][C:4]([CH3:5])([CH3:6])[CH3:7])[N:8]1[CH2:9][CH2:10][CH:11]([CH:14]=[O:15])[CH2:12][CH2:13]1

Participants

5

Reactant 4

HCID 6344DichloromethaneHCID 2764081Tert-butyl 4-(hydroxymethyl)piperidine-1-carboxylateHCID 4989215PyridiniumHCID 178418299HCID 178418299, compound

Product 1

HCID 1514430tert-Butyl 4-formylpiperidine-1-carboxylate

Sources & evidence

ORD record
ord-f68af55839674de0b99e9751ef5515d6
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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