→ HCID 10873182, compound

HRID 962331Notes

Reaction equation

HRID 962331 reaction equation
CC(=O)CC(=O)OCc1ccccc1.CC(=O)O.CCO.CNC(N)=O.O.O=Cc1cccc(Cl)c1Cl.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.[Yb+3]>>CC1=C(C(=O)OCc2ccccc2)C(c2cccc(Cl)c2Cl)NC(=O)N1C

Participants

7

Reactant 0

No Reactant data yet.

Product 1

HCID 10873182HCID 10873182, compoundYield 25%

Reagents, catalysts & solvents 6

HCID 176Acetic AcidOtherHCID 702EthanolOtherHCID 11719MethylureaOtherHCID 357452,3-DichlorobenzaldehydeOtherHCID 142266Benzyl acetoacetateOtherHCID 45075687Ytterbium(3+) trifluoromethanesulfonate--water (1/3/1)Other

Conditions

Temperature
120 °C

Workup

  1. waitNo procedure recorded
  2. additionNo procedure recorded
  3. waitNo procedure recorded
  4. filtrationKeep solid
  5. washNo procedure recorded
  6. dry in vacuumNo procedure recorded

Sources & evidence

ORD record
ord-1ec00231909b459a93191585054b303e
Source dataset
Microwave-assisted Biginelli Condensation Dataset
Original link
View source

Reaction notes

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