→ HCID 178436966, compound

HRID 962338Notes

Reaction equation

HRID 962338 reaction equation
CCC(=O)CC(=O)OC.CCO.CNC(N)=O.O.O=Cc1cccc(Cl)c1Cl.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.[Yb+3]>>CCC1=C(C(=O)OC)C(c2cccc(Cl)c2Cl)NC(=O)N1

Participants

6

Reactant 0

No Reactant data yet.

Product 1

HCID 178436966HCID 178436966, compoundYield 26%

Reagents, catalysts & solvents 5

HCID 702EthanolOther2×HCID 11719MethylureaOtherHCID 357452,3-DichlorobenzaldehydeOtherHCID 121699Methyl 3-oxovalerateOtherHCID 45075687Ytterbium(3+) trifluoromethanesulfonate--water (1/3/1)Other

Conditions

Temperature
120 °C

Workup

  1. waitNo procedure recorded
  2. additionNo procedure recorded
  3. waitNo procedure recorded
  4. filtrationKeep solid
  5. washNo procedure recorded
  6. dry in vacuumNo procedure recorded

Sources & evidence

ORD record
ord-043422534160457198b09d1c5a700fc0
Source dataset
Microwave-assisted Biginelli Condensation Dataset
Original link
View source

Reaction notes

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