HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylbenzophenone → 1,2-Bis(4-methylphenyl)-1,2-diphenyl-1,2-ethanediol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylbenzophenone | HCID 8652 | — |
| Catalyst | Acetic Acid | HCID 176 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | 1,2-Bis(4-methylphenyl)-1,2-diphenyl-1,2-ethanediol | HCID 4612495 | 98.7% |
Reaction Steps
0.04 g of acetic acid was added to 35.98 g of isopropyl alcohol, and 4.02 g of 4-methylbenzophenone was dissolved therein. To this solution, ultraviolet rays were irradiated by a high pressure mercury lamp (UVL-100HA, manufactured by Riko Kagaku Sangyo K.K.) to carry out the reaction for 4 hours. After the reaction, the solvent was distilled off to obtain 3.99 g of 1,2-bis(p-methylphenyl)-1,2-diphenyl-1,2-ethanediol (compound (C1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05759736 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-adf0930c4e5b4835ae0e21133440d648 |
| Source note | uspto-grants-1998_06 |