HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Acetoxybenzophenone → 1,2-Bis(p-acetoxyphenyl)-1,2-diphenyl-1,2-ethanediol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Acetoxybenzophenone | HCID 607716 | — |
| Catalyst | Acetic Acid | HCID 176 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | 1,2-Bis(p-acetoxyphenyl)-1,2-diphenyl-1,2-ethanediol | HCID 19084516 | 99.1% |
Reaction Steps
0.04 g of acetic acid was added to 35.98 g of isopropyl alcohol, and 4.02 g of 4-acetoxybenzophenone was dissolved therein. To this solution, ultraviolet rays were irradiated by a high pressure mercury lamp (UVL-100HA, manufactured by Riko Kagaku Sangyo K.K.) to carry out the reaction for 6 hours. After the reaction, the solvent was distilled off to obtain 4.00 g of 1,2-bis(p-acetoxyphenyl)-1,2-diphenyl-1,2-ethanediol (compound (C5)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05759736 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-a0f4d8b33ea947deb91d1479debd9a6b |
| Source note | uspto-grants-1998_06 |